<DIV>Hi Folmer,</DIV> <DIV> </DIV> <DIV>Thank you very much for your quickly reply.</DIV> <DIV> </DIV> <DIV>Actually, I didn't do any anomalous refinement by phenix.refine. I only used the default option.</DIV> <DIV> </DIV> <DIV>i checked the log file after refinement, it
seems that the annomalous flag is true. But i don't clear the anomalous be used or not.</DIV> <DIV> </DIV> <DIV>If yes, how i can report the number of observed reflections of refinment when PDB deposition. </DIV> <DIV><FONT size=4>I know the number of reflections for refinement and
experiment should be the number of all reflections which contains Friedel pairs.</FONT></DIV> <DIV>How i can make the <FONT size=4>SF file contains the Friedel pairs?</FONT><BR>
</DIV> <DIV> </DIV> <DIV>Thank you.</DIV> <DIV> </DIV> <DIV>Carl<BR>
<BR>
<B>Folmer Fredslund <folmerf@gmail.com></B> wrote:</DIV> <BLOCKQUOTE class=replbq style="PADDING-LEFT: 5px; MARGIN-LEFT: 5px; BORDER-LEFT: #1010ff 2px solid">Dear Carl,<BR>
<BR>
This might be an issue of whether you use the data as anomalous or<BR>
not. If the anomalous pairs are kept seperate then you will get<BR>
roughly twice the amount of data.<BR>
<BR>
I guess you could easily see if this is true by looking in the log<BR>
file or in the top of the resulting pdb file.<BR>
<BR>
Best regards,<BR>
Folmer Fredslund<BR>
<BR>
2009/4/24 <CARLBLUESKY@YAHOO.CO.JP>:<BR>
> Hi all,<BR>
><BR>
> I have a problem with reflection numbers of phenix.refine.<BR>
><BR>
> I did the phenix.refine then i found that the number of observed reflections<BR>
> given for the refinement 75747 (48-2.85A) is greater than the number of<BR>
> observed reflections<BR>
> for the experiment 40434 (50-2.85A). It shoud be around 40000.<BR>
> .<BR>
> This is a peak of MAD data about 2.85A. I used the TLS parameters to refine<BR>
> the structure.<BR>
> I really don't know why because this is my first time use phenix to do<BR>
> refinement.<BR>
><BR>
> Any advice and suggestion are welcome!<BR>
> Thanks.<BR>
><BR>
> Carl<BR>
><BR>
><BR>
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