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    Hi Almudena,<br>
    <br>
    the error message tries to tell you that for (0, 0, 16) index
    corresponding R-free-flag(+) and R-free-flag(-) are different
    indicating that something must have gone wrong when you were
    manipulating the files or may be the original tool that you used to
    create R-free-flag did it incorrectly. <br>
    <br>
    Can you send me that MTZ file and also explain how you obtained it?<br>
    <br>
    Pavel<br>
    <br>
    <div class="moz-cite-prefix">On 3/20/15 7:06 AM, Almudena Ponce
      Salvatierra wrote:<br>
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cite="mid:CAOggArkLL+BASLwsOf9CbV7S++eVQis9MQfU+wzerK__JVjb6A@mail.gmail.com"
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                <div>Hi everyone, <br>
                  <br>
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                I have merged 3 mtz files into one and done successfully
                Molecular replacement with it. However when I try to
                refine, I get the following error message: "cctbx error:
                merge_equivalents_exact: imcompatible flags for hkl (0,
                0, 16) (mismatch between Friedel pairs). <br>
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              How can I fix this? <br>
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            Thank you very much in advance. <br>
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          Best, <br>
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        Almudena<br clear="all">
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                    -- <br>
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                      <div dir="ltr">Almudena Ponce-Salvatierra
                        <div>Macromolecular crystallography and Nucleic
                          acid chemistry</div>
                        <div>Max Planck Institute for Biophysical
                          Chemistry</div>
                        <div>Am Fassberg 11 37077 Göttingen</div>
                        <div>Germany</div>
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