Hi,

 There may be PDB files which shows different protonation  state of HIS, at least there is PDB file shows double protonated HIS. At which resolution of the crystal can allow us to distinguish different protonation states of HIS?

an example:

M. Blakeley, F. Ruiz, R. Cachau, I. Hazemann, F. Meilleur, A. Mitschler, S. Ginell, P. Afonine, O. Ventura, A. Cousido, M. Haertlein, A. Joachimiak, D. Myles & A. Podjarny. Quantum model of catalysis based on a mobile proton revealed by subatomic x-ray and neutron diffraction studies of h-aldose reductase. (2008). PNAS. 105, 1844-1848.

Pavel