Hi, we refined a structure in phenix.refine (dev-1810) and the R-factors are:
Final R-work = 0.3221, R-free = 0.3638
phenix.cc_star agrees:
phenix.cc_star com_001.pdb com_001.mtz \
f_obs_labels="F-obs,SIGF-obs" \
f_model_labels="F-model,PHIF-model" \
unmerged_data="xscale.hkl"
r_work: 0.322
r_free: 0.364
so does phenix.model_vs_data:
phenix.model_vs_data com_001.pdb com_001.mtz
r_work : 0.3221
r_free : 0.3638
sigma_cutoff : None
However, when I calculate the R-factors with sftools, I get a discrepancy between the phenix and sftools results:
sftools << eof
read com_001_f_model.mtz
Y
select col R_FREE_FLAGS > 0
correl col FOBS FMODEL
select invert
correl col FOBS FMODEL
quit
Y
eof
R-work: 33.6
R-free: 38.1
Does anyone perhaps know what causes this difference?
With best regards, Simon
PS: The structure is in spacegroup P212121 with strong pseudocentering tNCS (dimer in the asymmetric unit, native Patterson peak at 0.500 0.500 0.497). No indication for a P21 twin (L-test and refinement in P21 with twin law), not higher symmetry spacegroup I222 (alternating strong and weak reflections are visible in the diffraction patterns, resolved structural differences in the two protomers of the dimer). Two datasets from different beamlines. As might be expected, the R-factors after refinement are unusually high (e.g. 28/35 [conventional resolution cutoff at 3.1 A], 32/36 with Kay's CC cufoff at 2.6 A). I wanted to compare refinements between different programs to see how they cope with the unexpected bimodal amplitude distribution.