P.S.: If you decide to send me the file please do so to my email address and not to the whole bulletin board.
Pavel.


On 1/11/11 10:46 AM, Hasan Demirci wrote:
Dear Pavel,
I always use command line, below is the parameters I used for refinement of this structure

phenix.refine output.mtz Par.pdb strategy=individual_sites+group_adp+occupancies+tls tls.params modifications.cif Antibiotics.cif zn_link.params restraints_edits.params group_adp_refinement_mode=two_adp_groups_per_residue secondary_structure_restraints=true write_eff_file=false write_geo_file=false wxc_scale=0.15 main.number_of_macro_cycles=2 ramachandran_restraints=True

Thanks.

On Tue, Jan 11, 2011 at 12:32 PM, Pavel Afonine <[email protected]> wrote:
Hi Hasan,

it sounds like you set up the refinement parameters such that you do not refine B-factors at all. This is the only explanation I can come up.

Can you send some more details about the refinement you did:

- did you use command line or GUI
- send a parameter file
etc...

Pavel.


On 1/11/11 8:55 AM, Hasan Demirci wrote:
Hi,
I am trying to refine a structure with a bound ligand "PAR".
Unfortunately, input b-factor of the ligand and output values are matching exactly even tough I copied the ligand from a different structure.
I manually changed the occupancy of the ligand to see if it changes the b-factor but again B-factor didn't change.
Can someone help me to solve this issue?
Below, I attached the first four lines of the pdb after occupancy change.

input
"HETATM51786  C11 PAR V   1     140.982  67.469  10.830  1.00 58.13           C 
HETATM51787  O11 PAR V   1     140.549  68.782  10.389  1.00 58.13           O 
HETATM51788  C21 PAR V   1     139.714  66.811  11.362  1.00 58.13           C 
HETATM51789  N21 PAR V   1     138.632  66.819  10.352  1.00 58.13           N "

output
"HETATM51828  C11 PAR V   1     157.285 114.375 -64.249  0.80 58.13           C 
HETATM51829  O11 PAR V   1     157.335 115.251 -65.379  0.80 58.13           O 
HETATM51830  C21 PAR V   1     158.559 113.509 -64.364  0.80 58.13           C 
HETATM51831  N21 PAR V   1     159.738 114.342 -64.677  0.80 58.13           N" 


Thanks.

--
Hasan DeMirci, Ph.D.
Postdoctoral Fellow
Department of Molecular Biology, Cellular Biology & Biochemistry
Brown University
185 Meeting Street
Providence, RI    02912

(401) 863-3652 lab (SFH)
(401) 863-6124 lab (ship st)
(401) 226-7852 cell

[email protected]
[email protected]


_______________________________________________
phenixbb mailing list
[email protected]
http://phenix-online.org/mailman/listinfo/phenixbb




--
Hasan DeMirci, Ph.D.
Postdoctoral Fellow
Department of Molecular Biology, Cellular Biology & Biochemistry
Brown University
185 Meeting Street
Providence, RI    02912

(401) 863-3652 lab (SFH)
(401) 863-6124 lab (ship st)
(401) 226-7852 cell

[email protected]
[email protected]
_______________________________________________ phenixbb mailing list [email protected] http://phenix-online.org/mailman/listinfo/phenixbb