Hi all,
I was trying to solve the structure of a protein in several
different datasets using xds and phenix. I could solve the structure
from one dataset in space group P4. For another dataset, I could solve
the structure using the monomer of the structure I got from the first
dataset as search model and solve the structure in space group mC. For
the third dataset, in IDXREF.LP, the space group of the highest symmetry
is hp: 101.2,
101.3, 58.8, 90, 90, 120. According to Mathiews coefficient,
1 monomer is expected in the asymmetric unit. But I couldn't get the
molecular replacement solution using the same method as for the second
dataset. I also tried several other search models (eg. deletion of the
potential flexible region in the search model) and tried to find the
solution in all possible pointgroup. I also tried to process the data
in oC (C222), the space group of the second highest symmetry in
IDXREF.LP, but, still I could not get right molecular replacement
solution.�
I don't whether this
means that there is a big conformational change for the structure in
the third dataset or the space
group I use is not right.
Let me know if any of you would have any comments or suggestions for me.
Thank you so much!
Best,
Wei